Information card for entry 4084338

Structure parameters

• Formula: C46 H38 Co F6 N P3 Sb
• Calculated formula: C46 H38 Co F6 N P3 Sb
• Title of publication: Peripheral Methyl Activation in η4-1,2,3,4-Tetramethylcyclobutadienylcobalt Complexes: Template Synthesis and Subsequent Reactivity of Triphosphamacrocycles
• Authors of publication: Edwards, Peter G.; Kariuki, Benson M.; Newman, Paul D.; Zhang, Wenjian
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 19
• Pages of publication: 5440
• a: 29.7573 ± 0.0005 Å
• b: 14.1366 ± 0.0002 Å
• c: 19.5726 ± 0.0004 Å
• α: 90°
• β: 96.818 ± 0.001°
• γ: 90°
• Cell volume: 8175.3 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.106
• Residual factor for significantly intense reflections: 0.0728
• Weighted residual factors for significantly intense reflections: 0.1729
• Weighted residual factors for all reflections included in the refinement: 0.1938
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No