Information card for entry 4084373

Structure parameters

• Formula: C15 H19 Cl3 N6 Pd2
• Calculated formula: C15 H19 Cl3 N6 Pd2
• Title of publication: Dinuclear Palladium Complexes of Pyrazole-Bridged Bis(NHC) Ligands: A Delicate Balance between Normal and Abnormal Carbene Coordination
• Authors of publication: Guo, Tongxun; Dechert, Sebastian; Meyer, Franc
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 19
• Pages of publication: 5145
• a: 8.5497 ± 0.0003 Å
• b: 12.7222 ± 0.0004 Å
• c: 18.0747 ± 0.0006 Å
• α: 92.151 ± 0.003°
• β: 96.359 ± 0.003°
• γ: 99.425 ± 0.003°
• Cell volume: 1924.42 ± 0.11 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0368
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.0747
• Weighted residual factors for all reflections included in the refinement: 0.0774
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No