Information card for entry 4084379

Structure parameters

• Formula: C19 H33 Cl2 N3 Si
• Calculated formula: C19 H33 Cl2 N3 Si
• SMILES: [SiH]1(Cl)(Cl)[N](=C(N1C(C)(C)C)N(C)C)c1c(C(C)C)cccc1C(C)C
• Title of publication: From Unsymmetrically Substituted Benzamidinato and Guanidinato Dichlorohydridosilanes to Novel Hydrido N-Heterocyclic Silylene Iron Complexes
• Authors of publication: Blom, Burgert; Pohl, Markus; Tan, Gengwen; Gallego, Daniel; Driess, Matthias
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 19
• Pages of publication: 5272
• a: 9.1949 ± 0.0001 Å
• b: 15.7363 ± 0.0001 Å
• c: 15.1115 ± 0.0001 Å
• α: 90°
• β: 93.372 ± 0.001°
• γ: 90°
• Cell volume: 2182.75 ± 0.03 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.028
• Residual factor for significantly intense reflections: 0.0266
• Weighted residual factors for significantly intense reflections: 0.0735
• Weighted residual factors for all reflections included in the refinement: 0.0745
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No