Information card for entry 4084441

Structure parameters

• Formula: C22 H31 Cl S Sn
• Calculated formula: C22 H31 Cl S Sn
• Title of publication: Synthetic, Structural, and Spectroscopic Studies of Sterically Crowded Tin‒Chalcogen Acenaphthenes
• Authors of publication: Athukorala Arachchige, Kasun S.; Diamond, Louise M.; Knight, Fergus R.; Lechner, Marie-Luise; Slawin, Alexandra M. Z.; Woollins, J. Derek
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 21
• Pages of publication: 6089
• a: 9.627 ± 0.002 Å
• b: 10.451 ± 0.003 Å
• c: 11.881 ± 0.003 Å
• α: 94.473 ± 0.007°
• β: 111.675 ± 0.008°
• γ: 95.075 ± 0.007°
• Cell volume: 1098.6 ± 0.5 ų
• Cell temperature: 125 K
• Ambient diffraction temperature: 125 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for all reflections included in the refinement: 0.103
• Goodness-of-fit parameter for all reflections included in the refinement: 0.899
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No