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Information card for entry 4084486
Preview
Coordinates | 4084486.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H37 F6 N2 Ni O P2 Sb |
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Calculated formula | C21 H37 F6 N2 Ni O P2 Sb |
SMILES | [Ni]12([P](N(c3c2c(N([P]1(C(C)C)C(C)C)C)ccc3)C)(C(C)C)C(C)C)C#[O].[Sb](F)(F)([F-])(F)(F)F |
Title of publication | Synthesis and Reactivity of Four- and Five-Coordinate Low-Spin Cobalt(II) PCP Pincer Complexes and Some Nickel(II) Analogues |
Authors of publication | Murugesan, Sathiyamoorthy; Stöger, Berthold; Carvalho, Maria Deus; Ferreira, Liliana P.; Pittenauer, Ernst; Allmaier, Günter; Veiros, Luis F.; Kirchner, Karl |
Journal of publication | Organometallics |
Year of publication | 2014 |
Pages of publication | 141009125933001 |
a | 14.6254 ± 0.0012 Å |
b | 8.4029 ± 0.0007 Å |
c | 23.161 ± 0.002 Å |
α | 90° |
β | 105.928 ± 0.002° |
γ | 90° |
Cell volume | 2737.1 ± 0.4 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0355 |
Residual factor for significantly intense reflections | 0.0264 |
Weighted residual factors for significantly intense reflections | 0.0323 |
Weighted residual factors for all reflections included in the refinement | 0.0332 |
Goodness-of-fit parameter for significantly intense reflections | 1.82 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.7 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4084486.html
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