Information card for entry 4084526

Structure parameters

• Formula: C24 H43 B F4 Fe N O3 P3
• Calculated formula: C24 H43 B F4 Fe N O3 P3
• Title of publication: Activation of Dihydrogen and Silanes by Cationic Iron Bis(phosphinite) Pincer Complexes
• Authors of publication: Bhattacharya, Papri; Krause, Jeanette A.; Guan, Hairong
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 21
• Pages of publication: 6113
• a: 17.939 ± 0.004 Å
• b: 11.161 ± 0.002 Å
• c: 16.404 ± 0.004 Å
• α: 90°
• β: 116.835 ± 0.003°
• γ: 90°
• Cell volume: 2930.7 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0527
• Residual factor for significantly intense reflections: 0.0338
• Weighted residual factors for significantly intense reflections: 0.0755
• Weighted residual factors for all reflections included in the refinement: 0.0824
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.7749 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No