Information card for entry 4084534

Structure parameters

• Formula: C18 H18 Fe N2 O2 S2 Si2
• Calculated formula: C18 H16 Fe N2 O2 S2 Si2
• Title of publication: Disilaferracycle Dicarbonyl Complex Containing Weakly Coordinated η2-(H-Si) Ligands: Application to C‒H Functionalization of Indoles and Arenes
• Authors of publication: Sunada, Yusuke; Soejima, Hiroe; Nagashima, Hideo
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 21
• Pages of publication: 5936
• a: 11.089 ± 0.003 Å
• b: 13.174 ± 0.004 Å
• c: 14.645 ± 0.004 Å
• α: 90°
• β: 91.371 ± 0.005°
• γ: 90°
• Cell volume: 2138.8 ± 1 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0642
• Weighted residual factors for all reflections included in the refinement: 0.1853
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No