Information card for entry 4084619

Structure parameters

• Formula: C28 H30 F3 N3 O2 Si Sn
• Calculated formula: C28 H30 F3 N3 O2 Si Sn
• SMILES: [Sn]12(OC(=CC(=[O]1)C(F)(F)F)c1ccccc1)[N](=C(N[Si](C)(C)C)N2c1ccc(cc1)C)c1ccc(cc1)C
• Title of publication: Reactivity of Tin(II) Guanidinate with 1,2- and 1,3-Diones: Oxidative Cycloaddition or Ligand Substitution ?
• Authors of publication: Chlupatý, Tomáš; Růžičková, Zdeňka; Horáček, Michal; Merna, Jan; Alonso, Mercedes; De Proft, Frank; Růžička, Aleš
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2202
• a: 11.043 ± 0.0004 Å
• b: 11.5469 ± 0.0007 Å
• c: 11.8801 ± 0.0006 Å
• α: 100.708 ± 0.004°
• β: 101.886 ± 0.004°
• γ: 102.09 ± 0.004°
• Cell volume: 1407.4 ± 0.13 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0252
• Residual factor for significantly intense reflections: 0.0219
• Weighted residual factors for significantly intense reflections: 0.0548
• Weighted residual factors for all reflections included in the refinement: 0.058
• Goodness-of-fit parameter for all reflections included in the refinement: 1.13
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No