Information card for entry 4084624

Structure parameters

• Formula: C48 H74 N2 O2 P4 Zn2
• Calculated formula: C48 H74 N2 O2 P4 Zn2
• Title of publication: Structures and CO2Reactivity of Zinc Complexes of Bis(diisopropyl-) and Bis(diphenylphosphino)amines
• Authors of publication: Dickie, Diane A.; Kemp, Richard A.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 22
• Pages of publication: 6511
• a: 19.2697 ± 0.0007 Å
• b: 11.6675 ± 0.0005 Å
• c: 22.8911 ± 0.0009 Å
• α: 90°
• β: 103.908 ± 0.002°
• γ: 90°
• Cell volume: 4995.7 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0696
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.1206
• Weighted residual factors for all reflections included in the refinement: 0.1269
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No