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Information card for entry 4084632
Preview
Coordinates | 4084632.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C26 H42 Br2 Ni O4 P2 |
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Calculated formula | C26 H42 Br2 Ni O4 P2 |
Title of publication | Ortho Derivatization of Phenols through C‒H Nickelation: Synthesis, Characterization, and Reactivities of Ortho-Nickelated Phosphinite Complexes |
Authors of publication | Vabre, Boris; Deschamps, Félix; Zargarian, Davit |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 22 |
Pages of publication | 6623 |
a | 9.0321 ± 0.0002 Å |
b | 11.04 ± 0.0003 Å |
c | 15.7 ± 0.0004 Å |
α | 102.066 ± 0.001° |
β | 96.868 ± 0.001° |
γ | 96.906 ± 0.001° |
Cell volume | 1502.84 ± 0.07 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0404 |
Residual factor for significantly intense reflections | 0.0403 |
Weighted residual factors for significantly intense reflections | 0.1067 |
Weighted residual factors for all reflections included in the refinement | 0.1067 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.197 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4084632.html
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Users of the data should acknowledge the original authors of the
structural data.