Information card for entry 4084686

Structure parameters

• Formula: C79 H71 Cl3 N O2.5 W
• Calculated formula: C79 H71 Cl3 N O2.5 W
• Title of publication: Synthesis of Tungsten Imido Alkylidene Complexes that Contain an Electron-Withdrawing Imido Ligand.
• Authors of publication: Axtell, Jonathan C.; Schrock, Richard R.; Müller, Peter; Smith, Stacey J.; Hoveyda, Amir H.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 19
• Pages of publication: 5342 - 5348
• a: 12.8493 ± 0.0018 Å
• b: 13.6749 ± 0.0019 Å
• c: 20.269 ± 0.003 Å
• α: 87.484 ± 0.003°
• β: 88.749 ± 0.003°
• γ: 69.065 ± 0.003°
• Cell volume: 3323.1 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.0686
• Weighted residual factors for all reflections included in the refinement: 0.075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No