Information card for entry 4084772

Structure parameters

• Formula: C70 H84 Al4 N10 O6 Sm2
• Calculated formula: C70 H84 Al4 N10 O6 Sm2
• Title of publication: Formation of a Heterometallic AlIII/SmIIIComplex Involving a Novel [EtAl(2-py)2O]2‒Ligand (2-py = 2-Pyridyl)
• Authors of publication: García-Rodríguez, Raúl; Simmonds, Hayley R.; Wright, Dominic S.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 24
• Pages of publication: 7113
• a: 12.7369 ± 0.0001 Å
• b: 13.0219 ± 0.0002 Å
• c: 13.3823 ± 0.0003 Å
• α: 105.862 ± 0.001°
• β: 94.212 ± 0.001°
• γ: 118.289 ± 0.001°
• Cell volume: 1825.28 ± 0.06 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0595
• Residual factor for significantly intense reflections: 0.0381
• Weighted residual factors for significantly intense reflections: 0.0848
• Weighted residual factors for all reflections included in the refinement: 0.0915
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No