Information card for entry 4084777

Structure parameters

• Formula: C33 H48 Ni O3 P2 Si
• Calculated formula: C33 H48 Ni O3 P2 Si
• Title of publication: POCOP-Ligated Nickel Siloxide Complexes: Syntheses, Characterization, and Reactivities
• Authors of publication: Hao, Jingjun; Vabre, Boris; Zargarian, Davit
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 22
• Pages of publication: 6568
• a: 10.8571 ± 0.0002 Å
• b: 15.7956 ± 0.0003 Å
• c: 19.8942 ± 0.0004 Å
• α: 90°
• β: 99.974 ± 0.001°
• γ: 90°
• Cell volume: 3360.18 ± 0.11 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0354
• Residual factor for significantly intense reflections: 0.0333
• Weighted residual factors for significantly intense reflections: 0.091
• Weighted residual factors for all reflections included in the refinement: 0.0931
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No