Information card for entry 4084779

Structure parameters

• Formula: C15 H33 N3 Ni O2 P2
• Calculated formula: C15 H33 N3 Ni O2 P2
• Title of publication: POCOP-Ligated Nickel Siloxide Complexes: Syntheses, Characterization, and Reactivities
• Authors of publication: Hao, Jingjun; Vabre, Boris; Zargarian, Davit
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 22
• Pages of publication: 6568
• a: 8.4288 ± 0.0006 Å
• b: 17.2331 ± 0.0012 Å
• c: 14.3787 ± 0.001 Å
• α: 90°
• β: 98.195 ± 0.003°
• γ: 90°
• Cell volume: 2067.2 ± 0.3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0329
• Residual factor for significantly intense reflections: 0.0323
• Weighted residual factors for significantly intense reflections: 0.0917
• Weighted residual factors for all reflections included in the refinement: 0.0923
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No