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Information card for entry 4084910
Preview
Coordinates | 4084910.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H50 P2 Pd |
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Calculated formula | C22 H50 P2 Pd |
Title of publication | Combining the Reactivity Properties of PCy3and PtBu3into a Single Ligand, P(iPr)(tBu)2. Reaction via Mono- or Bisphosphine Palladium(0) Centers and Palladium(I) Dimer Formation |
Authors of publication | Proutiere, Fabien; Lyngvi, Eirik; Aufiero, Marialuisa; Sanhueza, Italo A.; Schoenebeck, Franziska |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 23 |
Pages of publication | 6879 |
a | 8.036 ± 0.003 Å |
b | 8.385 ± 0.003 Å |
c | 11.704 ± 0.004 Å |
α | 98.158 ± 0.016° |
β | 103.103 ± 0.018° |
γ | 117.742 ± 0.016° |
Cell volume | 651.2 ± 0.4 Å3 |
Cell temperature | 100 ± 0.2 K |
Ambient diffraction temperature | 100 ± 0.2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0634 |
Residual factor for significantly intense reflections | 0.0436 |
Weighted residual factors for significantly intense reflections | 0.1048 |
Weighted residual factors for all reflections included in the refinement | 0.1156 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.054 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4084910.html
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