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Information card for entry 4084915
Preview
Coordinates | 4084915.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C39 H34 B2 F8 P2 |
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Calculated formula | C39 H34 B2 F8 P2 |
Title of publication | Synthesis of Phosphonium-Substituted Vinylidene Complexes from [HC\τb CCH2PPh3]+: Exploring the Competition between Allene and Vinylidene Formation. |
Authors of publication | Smith, Elizabeth J.; Pridmore, Natalie E.; Whitwood, Adrian C.; Lynam, Jason M. |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 24 |
Pages of publication | 7260 |
a | 9.9081 ± 0.0004 Å |
b | 13.7516 ± 0.0007 Å |
c | 14.6581 ± 0.0008 Å |
α | 65.358 ± 0.005° |
β | 75.008 ± 0.004° |
γ | 83.678 ± 0.004° |
Cell volume | 1753.52 ± 0.17 Å3 |
Cell temperature | 110.05 ± 0.1 K |
Ambient diffraction temperature | 110.05 ± 0.1 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0981 |
Residual factor for significantly intense reflections | 0.0765 |
Weighted residual factors for significantly intense reflections | 0.1706 |
Weighted residual factors for all reflections included in the refinement | 0.1828 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.079 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4084915.html
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Users of the data should acknowledge the original authors of the
structural data.