Crystallography Open Database

Information card for entry 4084949

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Coordinates	4084949.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C59 H58 B F24 Ir P2
Calculated formula	C59 H58 B F24 Ir P2
Title of publication	Rhodium and Iridium Complexes of Bulky Tertiary Phosphine Ligands. Searching for Isolable Cationic MIIIAlkylidenes
Authors of publication	Campos, Jesús; Carmona, Ernesto
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	11
Pages of publication	2212
a	12.3738 ± 0.0001 Å
b	13.0143 ± 0.0001 Å
c	18.6831 ± 0.0002 Å
α	88.945 ± 0.001°
β	80.381 ± 0.001°
γ	86.717 ± 0.001°
Cell volume	2961.37 ± 0.05 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.033
Residual factor for significantly intense reflections	0.0317
Weighted residual factors for significantly intense reflections	0.0762
Weighted residual factors for all reflections included in the refinement	0.0771
Goodness-of-fit parameter for all reflections included in the refinement	1.19
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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