Information card for entry 4084983

Structure parameters

• Formula: C24 H18 Cl2 P Sb
• Calculated formula: C24 H18 Cl2 P Sb
• SMILES: C1Cc2c3c1ccc1c3c(cc2)[P](c2ccccc2)(c2ccccc2)[Sb]1(Cl)Cl
• Title of publication: Probing Donor‒Acceptor Interactions inperi-Substituted Diphenylphosphinoacenaphthyl‒Element Dichlorides of Group 13 and 15 Elements
• Authors of publication: Hupf, Emanuel; Lork, Enno; Mebs, Stefan; Chęcińska, Lilianna; Beckmann, Jens
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 24
• Pages of publication: 7247
• a: 12.497 ± 0.003 Å
• b: 9.194 ± 0.003 Å
• c: 19.193 ± 0.004 Å
• α: 90°
• β: 106.221 ± 0.011°
• γ: 90°
• Cell volume: 2117.4 ± 1 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0359
• Residual factor for significantly intense reflections: 0.0304
• Weighted residual factors for significantly intense reflections: 0.0706
• Weighted residual factors for all reflections included in the refinement: 0.0729
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No