Information card for entry 4085238

Structure parameters

• Formula: C31 H36 Cl2 Fe Ge N2 O4
• Calculated formula: C31 H36 Cl2 Fe Ge N2 O4
• SMILES: C(#[O])[Fe](C#[O])(C#[O])(C#[O])[Ge](=C1N(C=CN1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)(Cl)Cl
• Title of publication: Iron Complexes with Stabilized Germylenes: Syntheses and Characterizations
• Authors of publication: El Ezzi, Mohammad; Kocsor, Tibor-Gabor; D’Accriscio, Florian; Madec, David; Mallet-Ladeira, Sonia; Castel, Annie
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 3
• Pages of publication: 571
• a: 33.936 ± 0.005 Å
• b: 39.39 ± 0.006 Å
• c: 10.4595 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 13982 ± 4 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.1038
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.0898
• Weighted residual factors for all reflections included in the refinement: 0.119
• Goodness-of-fit parameter for all reflections included in the refinement: 0.598
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No