Information card for entry 4085248

Structure parameters

• Formula: C15 H36 K N Si2
• Calculated formula: C15 H36 K N Si2
• Title of publication: Homoleptic Trigonal Planar Lanthanide Complexes Stabilized by Superbulky Silylamide Ligands
• Authors of publication: Goodwin, Conrad A. P.; Joslin, Kristian C.; Lockyer, Selena J.; Formanuik, Alasdair; Morris, Gareth A.; Ortu, Fabrizio; Vitorica-Yrezabal, Iñigo. J.; Mills, David P.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2314
• a: 11.8947 ± 0.0012 Å
• b: 12.0009 ± 0.0014 Å
• c: 15.3957 ± 0.0016 Å
• α: 90°
• β: 109.225 ± 0.011°
• γ: 90°
• Cell volume: 2075.1 ± 0.4 ų
• Cell temperature: 139 ± 15 K
• Ambient diffraction temperature: 139 ± 15 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1598
• Residual factor for significantly intense reflections: 0.0847
• Weighted residual factors for significantly intense reflections: 0.1097
• Weighted residual factors for all reflections included in the refinement: 0.146
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No