Information card for entry 4085267

Structure parameters

• Formula: C65 H69.5 Co N3 O0.75 Si
• Calculated formula: C65 H69.5 Co N3 O0.75 Si
• Title of publication: Low-Coordinate Cobalt(I) Complexes Stabilized by an Extremely Bulky Amide Ligand
• Authors of publication: Hicks, Jamie; Jones, Cameron
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2118
• a: 12.495 ± 0.003 Å
• b: 19.107 ± 0.004 Å
• c: 24.377 ± 0.005 Å
• α: 105.22 ± 0.03°
• β: 89.89 ± 0.03°
• γ: 104.4 ± 0.03°
• Cell volume: 5427 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0725
• Residual factor for significantly intense reflections: 0.0583
• Weighted residual factors for significantly intense reflections: 0.146
• Weighted residual factors for all reflections included in the refinement: 0.1553
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.7109 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No