Information card for entry 4085273

Structure parameters

• Formula: C24 H23 Cl2 N2 Sb
• Calculated formula: C24 H23 Cl2 N2 Sb
• SMILES: [Sb]12(Cl)(Cl)[N](=Cc3cccc(c23)C=[N]1c1c(C)cccc1C)c1c(cccc1C)C
• Title of publication: Reactivity of N,C,N-Chelated Antimony(III) and Bismuth(III) Chlorides with Lithium Reagents: Addition vs Substitution
• Authors of publication: Vránová, Iva; Jambor, Roman; Růžička, Aleš; Jirásko, Robert; Dostál, Libor
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 2
• Pages of publication: 534
• a: 16.7321 ± 0.0019 Å
• b: 16.7321 ± 0.0019 Å
• c: 7.963 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2229.3 ± 0.4 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 5
• Space group number: 81
• Hermann-Mauguin space group symbol: P -4
• Hall space group symbol: P -4
• Residual factor for all reflections: 0.0504
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.0881
• Weighted residual factors for all reflections included in the refinement: 0.0917
• Goodness-of-fit parameter for all reflections included in the refinement: 1.145
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No