Information card for entry 4085277

Structure parameters

• Formula: C36 H33 N2 Sb
• Calculated formula: C36 H33 N2 Sb
• SMILES: [Sb]1(c2ccccc2)c2c(/C=N/c3c(cccc3C)C)cccc2C(N1c1c(C)cccc1C)c1ccccc1
• Title of publication: Reactivity of N,C,N-Chelated Antimony(III) and Bismuth(III) Chlorides with Lithium Reagents: Addition vs Substitution
• Authors of publication: Vránová, Iva; Jambor, Roman; Růžička, Aleš; Jirásko, Robert; Dostál, Libor
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 2
• Pages of publication: 534
• a: 10.659 ± 0.0013 Å
• b: 15.7679 ± 0.0019 Å
• c: 17.727 ± 0.0011 Å
• α: 90°
• β: 92.542 ± 0.007°
• γ: 90°
• Cell volume: 2976.4 ± 0.5 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0664
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.0894
• Weighted residual factors for all reflections included in the refinement: 0.1084
• Goodness-of-fit parameter for all reflections included in the refinement: 1.12
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No