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Information card for entry 4085322
Preview
Coordinates | 4085322.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C29 H38 Cl0.5 N2.5 Pd |
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Calculated formula | C29 H38 Cl0.5 N2.5 Pd |
Title of publication | Effect of 2-Substituents on Allyl-Supported Precatalysts for the Suzuki‒Miyaura Reaction: Relating Catalytic Efficiency to the Stability of Palladium(I) Bridging Allyl Dimers |
Authors of publication | Hruszkewycz, Damian P.; Guard, Louise M.; Balcells, David; Feldman, Nicola; Hazari, Nilay; Tilset, Mats |
Journal of publication | Organometallics |
Year of publication | 2015 |
Journal volume | 34 |
Journal issue | 1 |
Pages of publication | 381 |
a | 19.7597 ± 0.0013 Å |
b | 11.8025 ± 0.0002 Å |
c | 24.259 ± 0.003 Å |
α | 90° |
β | 108.371 ± 0.007° |
γ | 90° |
Cell volume | 5369.2 ± 0.8 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | I 1 2/a 1 |
Hall space group symbol | -I 2ya |
Residual factor for all reflections | 0.1055 |
Residual factor for significantly intense reflections | 0.097 |
Weighted residual factors for significantly intense reflections | 0.2202 |
Weighted residual factors for all reflections included in the refinement | 0.2239 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.29 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4085322.html
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