Information card for entry 4085477

Structure parameters

• Formula: C36 H58 Ge2 N4 Na2 O4
• Calculated formula: C36 H58 Ge2 N4 Na2 O4
• SMILES: [Ge]1[N]2(c3ccccc3N1C(C)(C)C)[Na]([O]1CCCC1)([O]1CCCC1)[N]1([Ge]N(c3c1cccc3)C(C)(C)C)[Na]2([O]1CCCC1)[O]1CCCC1
• Title of publication: Protic N-Heterocyclic Germylenes and Stannylenes: Synthesis and Reactivity
• Authors of publication: Krupski, Sergei; Schulte to Brinke, Christian; Koppetz, Hannah; Hepp, Alexander; Hahn, F. Ekkehardt
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2624
• a: 8.6146 ± 0.0003 Å
• b: 12.5729 ± 0.0004 Å
• c: 18.9466 ± 0.0005 Å
• α: 90°
• β: 93.006 ± 0.002°
• γ: 90°
• Cell volume: 2049.29 ± 0.11 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.071
• Residual factor for significantly intense reflections: 0.0413
• Weighted residual factors for significantly intense reflections: 0.1173
• Weighted residual factors for all reflections included in the refinement: 0.1429
• Goodness-of-fit parameter for all reflections included in the refinement: 1.123
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No