Information card for entry 4085498

Structure parameters

• Common name: Compound 9
• Formula: C65 H77 Cr2 I N4
• Calculated formula: C65 H77 Cr2 I N4
• Title of publication: Low-Valent Aminopyridinato Chromium Methyl Complexes via Reductive Alkylation and via Oxidative Addition of Iodomethane by a Cr‒Cr Quintuple Bond
• Authors of publication: Noor, Awal; Schwarz, Stefan; Kempe, Rhett
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2122
• a: 10.4779 ± 0.0008 Å
• b: 11.8984 ± 0.0008 Å
• c: 13.6997 ± 0.0009 Å
• α: 65.129 ± 0.005°
• β: 89.534 ± 0.006°
• γ: 69.427 ± 0.005°
• Cell volume: 1431 ± 0.2 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1391
• Residual factor for significantly intense reflections: 0.0595
• Weighted residual factors for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections included in the refinement: 0.1205
• Goodness-of-fit parameter for all reflections included in the refinement: 0.795
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No