Information card for entry 4085630

Structure parameters

• Formula: C73 H71 B2 Cl2 F8 N5 Os P2
• Calculated formula: C72 H69 B2 F8 N5 Os P2
• Title of publication: Bis(pyridylimino)isoindolato (BPI) Osmium Complexes: Structural Chemistry and Reactivity
• Authors of publication: Müller, Astrid L.; Wadepohl, Hubert; Gade, Lutz H.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 12
• Pages of publication: 2810
• a: 12.407 ± 0.005 Å
• b: 15.235 ± 0.007 Å
• c: 18.64 ± 0.009 Å
• α: 108.001 ± 0.008°
• β: 98.002 ± 0.012°
• γ: 95.292 ± 0.011°
• Cell volume: 3284 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0386
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.0691
• Weighted residual factors for all reflections included in the refinement: 0.0763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No