Information card for entry 4085647

Structure parameters

• Formula: C53 H53 Cl4 Cu4 N8 O9
• Calculated formula: C53 H44 Cl4 Cu4 N8 O9
• Title of publication: Synthesis of Multinuclear Copper Complexes Bridged by Diquinolylamidinates and Their Application to Copper-Catalyzed Coupling of Terminal Alkynes and Aryl, Allyl, and Benzyl Halides
• Authors of publication: Nakane, Takayuki; Tanioka, Yuta; Tsukada, Naofumi
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 7
• Pages of publication: 1191
• a: 14.12 ± 0.005 Å
• b: 25.357 ± 0.007 Å
• c: 24.651 ± 0.009 Å
• α: 90°
• β: 131.715 ± 0.004°
• γ: 90°
• Cell volume: 6588 ± 4 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0694
• Weighted residual factors for all reflections included in the refinement: 0.1532
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No