Information card for entry 4085657

Structure parameters

• Formula: C36 H48 N2 Pb
• Calculated formula: C36 H48 N2 Pb
• Title of publication: β-Diketiminato Organolead Complexes: Structures,207Pb NMR, and Hammett Correlations
• Authors of publication: Taylor, Morgan J.; Coakley, Emma J.; Coles, Martyn P.; Cox, Hazel; Fulton, J. Robin
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2515
• a: 16.2236 ± 0.0002 Å
• b: 20.5353 ± 0.0002 Å
• c: 9.938 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3310.91 ± 0.06 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0309
• Residual factor for significantly intense reflections: 0.0262
• Weighted residual factors for significantly intense reflections: 0.0619
• Weighted residual factors for all reflections included in the refinement: 0.0639
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No