Information card for entry 4085683

Structure parameters

• Common name: K^3^(2-triphenylphosphinimine-5-methylbenzenesulfonate) palladium(4-tbutylpyridine)
• Chemical name: K^3^(2-triphenylphosphinimine-5-methylbenzenesulfonate) palladium(4-tbutylpyridine)
• Formula: C43 H23 N2 O3 P Pd S
• Calculated formula: C43 H23 N2 O3 P Pd S
• Title of publication: Synthesis and Reactivity of Neutral Palladium(II) Alkyl Complexes that Contain Phosphinimine-Arenesulfonate Ligands
• Authors of publication: Burns, Christopher T.; Shang, Suisheng; Mashuta, Mark S.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 10
• Pages of publication: 1844
• a: 9.3572 ± 0.0006 Å
• b: 11.8341 ± 0.0008 Å
• c: 18.5228 ± 0.0014 Å
• α: 87.01 ± 0.006°
• β: 87.005 ± 0.006°
• γ: 69.223 ± 0.006°
• Cell volume: 1913.9 ± 0.2 ų
• Cell temperature: 99.95 ± 0.1 K
• Ambient diffraction temperature: 99.95 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0694
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1071
• Weighted residual factors for all reflections included in the refinement: 0.1151
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No