Information card for entry 4085802

Structure parameters

• Formula: C56 H50 B O2 P2 Pd
• Calculated formula: C56 H50 B O2 P2 Pd
• Title of publication: Synthesis and Reactivity of Palladium Complexes Featuring a Diphosphinoborane Ligand
• Authors of publication: Schindler, Tobias; Lux, Marcel; Peters, Marius; Scharf, Lennart T.; Osseili, Hassan; Maron, Laurent; Tauchert, Michael E.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 10
• Pages of publication: 1978
• a: 9.874 ± 0.002 Å
• b: 14.424 ± 0.003 Å
• c: 18.105 ± 0.004 Å
• α: 66.69 ± 0.03°
• β: 77.83 ± 0.03°
• γ: 71.49 ± 0.03°
• Cell volume: 2234.8 ± 1 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0508
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0951
• Weighted residual factors for all reflections included in the refinement: 0.1017
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MOKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No