Information card for entry 4086125

Structure parameters

• Formula: C57 H129 F9 N3 O18 S3 Si15
• Calculated formula: C57 H129 F9 N3 O18 S3 Si15
• Title of publication: Oligosilanylsilatranes.
• Authors of publication: Aghazadeh Meshgi, Mohammad; Baumgartner, Judith; Marschner, Christoph
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 15
• Pages of publication: 3721 - 3731
• a: 21.03 ± 0.003 Å
• b: 10.2241 ± 0.0016 Å
• c: 45.503 ± 0.007 Å
• α: 90°
• β: 92.743 ± 0.003°
• γ: 90°
• Cell volume: 9773 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0905
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.1392
• Weighted residual factors for all reflections included in the refinement: 0.1508
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No