Information card for entry 4086144

Structure parameters

• Formula: C84 H117 Cl Ge O13 P2 Ru Si7
• Calculated formula: C84 H117 Cl Ge O13 P2 Ru Si7
• Title of publication: New Vinylgermanium Derivatives of Silsesquioxanes and Their Ruthenium Complexes—Synthesis, Structure, and Reactivity
• Authors of publication: Frąckowiak, Dawid; Żak, Patrycja; Spólnik, Grzegorz; Pyziak, Mikołaj; Marciniec, Bogdan
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 16
• Pages of publication: 3950
• a: 15.2168 ± 0.0006 Å
• b: 15.5813 ± 0.0006 Å
• c: 19.4687 ± 0.0006 Å
• α: 93.033 ± 0.003°
• β: 91.536 ± 0.003°
• γ: 102.934 ± 0.003°
• Cell volume: 4489 ± 0.3 ų
• Cell temperature: 130 ± 0.1 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0919
• Residual factor for significantly intense reflections: 0.0691
• Weighted residual factors for significantly intense reflections: 0.1902
• Weighted residual factors for all reflections included in the refinement: 0.2313
• Goodness-of-fit parameter for all reflections included in the refinement: 0.81
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No