Information card for entry 4086171

Structure parameters

• Common name: [Fe(CNSi Me3)2(NPPN)](SbF6)2
• Formula: C48 H64 F12 Fe N4 P2 Sb2 Si2
• Calculated formula: C48 H64 F12 Fe N4 P2 Sb2 Si2
• Title of publication: Chiral Iron(II) NPPN Complexes: Synthesis and Application in the Asymmetric Strecker Reaction of Azomethine Imines
• Authors of publication: Huber, Raffael; Bigler, Raphael; Mezzetti, Antonio
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 13
• Pages of publication: 3374
• a: 11.2303 ± 0.0005 Å
• b: 11.2303 ± 0.0005 Å
• c: 44.95 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5669.1 ± 0.5 ų
• Cell temperature: 101 ± 2 K
• Ambient diffraction temperature: 101 ± 2 K
• Number of distinct elements: 8
• Space group number: 96
• Hermann-Mauguin space group symbol: P 43 21 2
• Hall space group symbol: P 4nw 2abw
• Residual factor for all reflections: 0.1143
• Residual factor for significantly intense reflections: 0.0744
• Weighted residual factors for significantly intense reflections: 0.1609
• Weighted residual factors for all reflections included in the refinement: 0.1738
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No