Information card for entry 4086224

Structure parameters

• Formula: C24 H72 N8 S4 Si8 Zn2
• Calculated formula: C24 H72 N8 S4 Si8 Zn2
• Title of publication: Synthesis and X-ray Crystal Structure of Diimidosulfinate Transition Metal Complexes
• Authors of publication: Bayram, Melike; Bläser, Dieter; Wölper, Christoph; Schulz, Stephan
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 13
• Pages of publication: 3421
• a: 19.1987 ± 0.0009 Å
• b: 12.6735 ± 0.0007 Å
• c: 20.0406 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4876.2 ± 0.5 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0739
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0752
• Weighted residual factors for all reflections included in the refinement: 0.088
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No