Information card for entry 4086228

Structure parameters

• Formula: C22 H58 Li2 N4 O2 S2 Si4
• Calculated formula: C22 H58 Li2 N4 O2 S2 Si4
• SMILES: [S]1([N]2([Si](C)(C)C)[Li]([O]3CCCC3)([N]=1[Si](C)(C)C)[N]1(S(=[N]([Si](C)(C)C)[Li]21[O]1CCCC1)C)[Si](C)(C)C)C
• Title of publication: Synthesis and X-ray Crystal Structure of Diimidosulfinate Transition Metal Complexes
• Authors of publication: Bayram, Melike; Bläser, Dieter; Wölper, Christoph; Schulz, Stephan
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 13
• Pages of publication: 3421
• a: 9.9253 ± 0.0005 Å
• b: 10.466 ± 0.0005 Å
• c: 10.483 ± 0.0005 Å
• α: 62.694 ± 0.002°
• β: 73.265 ± 0.002°
• γ: 67.081 ± 0.002°
• Cell volume: 883.24 ± 0.08 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0284
• Residual factor for significantly intense reflections: 0.0238
• Weighted residual factors for significantly intense reflections: 0.0645
• Weighted residual factors for all reflections included in the refinement: 0.0676
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No