Information card for entry 4086230

Structure parameters

• Formula: C22 H32 B3 La N2
• Calculated formula: C22 H32 B3 La N2
• Title of publication: Tris(boratabenzene) Lanthanum Complexes: Synthesis, Structure, and Reactivity
• Authors of publication: Wang, Chunhong; Leng, Xuebing; Chen, Yaofeng
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 13
• Pages of publication: 3216
• a: 31.77 ± 0.003 Å
• b: 8.6243 ± 0.0007 Å
• c: 16.5042 ± 0.0013 Å
• α: 90°
• β: 93.061 ± 0.001°
• γ: 90°
• Cell volume: 4515.6 ± 0.7 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0196
• Residual factor for significantly intense reflections: 0.0165
• Weighted residual factors for significantly intense reflections: 0.0529
• Weighted residual factors for all reflections included in the refinement: 0.0553
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No