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Information card for entry 4086388
Preview
Coordinates | 4086388.cif |
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Original paper (by DOI) | HTML |
Formula | C23.92 H50.77 Ca I1.02 O4 Si0.98 |
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Calculated formula | C23.9144 H50.7646 Ca I1.0214 O4 Si0.9786 |
Title of publication | Trimethylsilylmethylcalcium Iodide, an Easily Accessible Grignard-Type Reagent of a Heavy Alkaline Earth Metal |
Authors of publication | Köhler, Mathias; Koch, Alexander; Görls, Helmar; Westerhausen, Matthias |
Journal of publication | Organometallics |
Year of publication | 2016 |
Journal volume | 35 |
Journal issue | 2 |
Pages of publication | 242 |
a | 17.6823 ± 0.0003 Å |
b | 17.4313 ± 0.0003 Å |
c | 10.0658 ± 0.0002 Å |
α | 90° |
β | 100.715 ± 0.001° |
γ | 90° |
Cell volume | 3048.44 ± 0.1 Å3 |
Cell temperature | 133 ± 2 K |
Ambient diffraction temperature | 133 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0252 |
Residual factor for significantly intense reflections | 0.0225 |
Weighted residual factors for significantly intense reflections | 0.0452 |
Weighted residual factors for all reflections included in the refinement | 0.0464 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4086388.html
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