Information card for entry 4086677

Structure parameters

• Formula: C27 H44 Cl Ge N2 Rh
• Calculated formula: C27 H44 Cl Ge N2 Rh
• SMILES: CC(C)(C)[N]1=C(c2ccccc2)N(C(C)(C)C)[Ge]1(C(C)(C)C)[Rh]123([CH]4=[CH]1CC[CH]2=[CH]3CC4)Cl
• Title of publication: Amidinatogermylene Metal Complexes as Homogeneous Catalysts in Alcoholic Media
• Authors of publication: Álvarez-Rodríguez, Lucía; Cabeza, Javier A.; Fernández-Colinas, José M.; García-Álvarez, Pablo; Polo, Diego
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 15
• Pages of publication: 2516
• a: 16.7872 ± 0.0002 Å
• b: 12.282 ± 0.0002 Å
• c: 13.9392 ± 0.0002 Å
• α: 90°
• β: 106.677 ± 0.002°
• γ: 90°
• Cell volume: 2753.1 ± 0.07 ų
• Cell temperature: 120 ± 1 K
• Ambient diffraction temperature: 120 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0428
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.0577
• Weighted residual factors for all reflections included in the refinement: 0.0626
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No