Information card for entry 4086815

Structure parameters

• Formula: C26 H21 N Si
• Calculated formula: C26 H21 N Si
• SMILES: [Si]1(c2c3ccccc3n(C)c2c2cc3ccccc3cc12)(c1ccccc1)C
• Title of publication: Catalytic Access to Indole-Fused Benzosiloles by 2-Fold Electrophilic C‒H Silylation with Dihydrosilanes
• Authors of publication: Omann, Lukas; Oestreich, Martin
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 36
• Journal issue: 4
• Pages of publication: 767
• a: 8.30541 ± 0.00006 Å
• b: 24.67353 ± 0.00018 Å
• c: 38.1106 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7809.77 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0366
• Residual factor for significantly intense reflections: 0.0325
• Weighted residual factors for significantly intense reflections: 0.0848
• Weighted residual factors for all reflections included in the refinement: 0.0884
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No