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Information card for entry 4086949
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Coordinates | 4086949.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C33 H60 B3 N |
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Calculated formula | C33 H60 B3 N |
Title of publication | Dynamic Exchange in Intramolecular Lewis Pairs with Multiple Lewis-Acidic Functions |
Authors of publication | Körte, Leif A.; Blomeyer, Sebastian; Peters, Jan-Hendrik; Mix, Andreas; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W. |
Journal of publication | Organometallics |
Year of publication | 2017 |
Journal volume | 36 |
Journal issue | 3 |
Pages of publication | 742 |
a | 8.4657 ± 0.0007 Å |
b | 13.0744 ± 0.0018 Å |
c | 14.2825 ± 0.0015 Å |
α | 75.75 ± 0.01° |
β | 80.154 ± 0.008° |
γ | 82.275 ± 0.009° |
Cell volume | 1502.6 ± 0.3 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0613 |
Residual factor for significantly intense reflections | 0.0476 |
Weighted residual factors for significantly intense reflections | 0.1266 |
Weighted residual factors for all reflections included in the refinement | 0.1323 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4086949.html
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Users of the data should acknowledge the original authors of the
structural data.