Information card for entry 4087153

Structure parameters

• Formula: C47 H62.15 P2 Pd Si
• Calculated formula: C47 H62.152 P2 Pd Si
• Title of publication: An Adaptable Chelating Diphosphine Ligand for the Stabilization of Palladium and Platinum Carbenes
• Authors of publication: Barrett, Brittany J.; Iluc, Vlad M.
• Journal of publication: Organometallics
• Year of publication: 2017
• Journal volume: 36
• Journal issue: 3
• Pages of publication: 730
• a: 9.7476 ± 0.0003 Å
• b: 13.374 ± 0.0005 Å
• c: 17.3877 ± 0.0006 Å
• α: 72.906 ± 0.001°
• β: 83.919 ± 0.001°
• γ: 81.841 ± 0.001°
• Cell volume: 2139.73 ± 0.13 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0286
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for significantly intense reflections: 0.0632
• Weighted residual factors for all reflections included in the refinement: 0.0643
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No