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Information card for entry 4087161
Preview
Coordinates | 4087161.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C54 H52 Fe P4 |
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Calculated formula | C54 H52 Fe P4 |
SMILES | [Fe]123([P](CC[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)([P](CC[P]2(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)[CH2]=[CH2]3 |
Title of publication | Straightforward Access to Stable, 16-Valence-Electron Phosphine-Stabilized Fe0 Olefin Complexes and Their Reactivity |
Authors of publication | Burcher, Benjamin; Sanders, Kevin J.; Benda, Ladislav; Pintacuda, Guido; Jeanneau, Erwann; Danopoulos, Andreas A.; Braunstein, Pierre; Olivier-Bourbigou, Hélène; Breuil, Pierre-Alain R. |
Journal of publication | Organometallics |
Year of publication | 2017 |
Journal volume | 36 |
Journal issue | 3 |
Pages of publication | 605 |
a | 23.275 ± 0.003 Å |
b | 10.8131 ± 0.0012 Å |
c | 17.896 ± 0.002 Å |
α | 90° |
β | 106.233 ± 0.013° |
γ | 90° |
Cell volume | 4324.4 ± 0.9 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.13 |
Residual factor for significantly intense reflections | 0.0918 |
Weighted residual factors for all reflections | 0.2907 |
Weighted residual factors for significantly intense reflections | 0.2506 |
Weighted residual factors for all reflections included in the refinement | 0.2907 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.9216 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4087161.html
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Users of the data should acknowledge the original authors of the
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