Zirconocene-Based Methods for the Preparation of BN-Indenes: Application to the Synthesis of 1,5-Dibora-4a,8a-diaza-1,2,3,5,6,7-hexaaryl-4,8-dimethyl-s-indacenes
Authors of publication
Morgan, Matthew M.; Patrick, Evan A.; Rautiainen, J. Mikko; Tuononen, Heikki M.; Piers, Warren E.; Spasyuk, Denis M.
Journal of publication
Organometallics
Year of publication
2017
a
12.6013 ± 0.0002 Å
b
14.2473 ± 0.0002 Å
c
15.7688 ± 0.0002 Å
α
63.993 ± 0.001°
β
86.318 ± 0.001°
γ
80.98 ± 0.001°
Cell volume
2512.88 ± 0.07 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0548
Residual factor for significantly intense reflections
0.0416
Weighted residual factors for significantly intense reflections
0.1051
Weighted residual factors for all reflections included in the refinement
0.1147
Goodness-of-fit parameter for all reflections included in the refinement
