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Information card for entry 4087203
Preview
Coordinates | 4087203.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H18 Cl3 O P Te |
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Calculated formula | C24 H18 Cl3 O P Te |
SMILES | [Te]1(Cl)(Cl)(Cl)c2ccc3c4c(CC3)ccc(P(=[O]1)(c1ccccc1)c1ccccc1)c24 |
Title of publication | Selective Oxidation and Functionalization of 6-Diphenylphosphinoacenaphthyl-5-tellurenyl Species 6-Ph2P-Ace-5-TeX (X = Mes, Cl, O3SCF3). Various Types of P‒E···Te(II,IV) Bonding Situations (E = O, S, Se) |
Authors of publication | Hupf, Emanuel; Do, Truong Giang; Nordheider, Andreas; Wehrhahn, Maren; Sanz Camacho, Paula; Ashbrook, Sharon E.; Lork, Enno; Slawin, Alexandra M. Z.; Mebs, Stefan; Woollins, J. Derek; Beckmann, Jens |
Journal of publication | Organometallics |
Year of publication | 2017 |
a | 9.2866 ± 0.0003 Å |
b | 9.5461 ± 0.0004 Å |
c | 14.5827 ± 0.0005 Å |
α | 96.029 ± 0.001° |
β | 98.025 ± 0.001° |
γ | 117.728 ± 0.001° |
Cell volume | 1111.6 ± 0.07 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0366 |
Residual factor for significantly intense reflections | 0.0275 |
Weighted residual factors for significantly intense reflections | 0.0599 |
Weighted residual factors for all reflections included in the refinement | 0.0639 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4087203.html
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Users of the data should acknowledge the original authors of the
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