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Information card for entry 4087205
Preview
Coordinates | 4087205.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H18 I3 O P Te |
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Calculated formula | C24 H18 I3 O P Te |
SMILES | [O]1[Te](I)(I)(I)c2c3c(P=1(c1ccccc1)c1ccccc1)ccc1CCc(c31)cc2 |
Title of publication | Selective Oxidation and Functionalization of 6-Diphenylphosphinoacenaphthyl-5-tellurenyl Species 6-Ph2P-Ace-5-TeX (X = Mes, Cl, O3SCF3). Various Types of P‒E···Te(II,IV) Bonding Situations (E = O, S, Se) |
Authors of publication | Hupf, Emanuel; Do, Truong Giang; Nordheider, Andreas; Wehrhahn, Maren; Sanz Camacho, Paula; Ashbrook, Sharon E.; Lork, Enno; Slawin, Alexandra M. Z.; Mebs, Stefan; Woollins, J. Derek; Beckmann, Jens |
Journal of publication | Organometallics |
Year of publication | 2017 |
a | 13.5535 ± 0.0004 Å |
b | 12.2415 ± 0.0003 Å |
c | 14.8388 ± 0.0004 Å |
α | 90° |
β | 93.301 ± 0.001° |
γ | 90° |
Cell volume | 2457.9 ± 0.12 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0185 |
Residual factor for significantly intense reflections | 0.0152 |
Weighted residual factors for significantly intense reflections | 0.0326 |
Weighted residual factors for all reflections included in the refinement | 0.0336 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.093 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4087205.html
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