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Information card for entry 4087207
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Coordinates | 4087207.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | AS-2 |
---|---|
Formula | C29 H26 N O5 P W |
Calculated formula | C29 H26 N O5 P W |
SMILES | [W]([PH](N1CCCCC1)C(c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])(C#[O])(C#[O])(C#[O])C#[O] |
Title of publication | 1,1′-Bifunctional Aminophosphane Complexes via N‒H Bond Insertions of a Li/Cl Phosphinidenoid Complex and First Studies on N/P Mono Functionalizations |
Authors of publication | Streubel, Rainer; Schmer, Alexander; Kyri, Andreas W.; Schnakenburg, Gregor |
Journal of publication | Organometallics |
Year of publication | 2017 |
a | 14.7592 ± 0.0005 Å |
b | 32.0367 ± 0.001 Å |
c | 11.2598 ± 0.0004 Å |
α | 90° |
β | 91.4175 ± 0.0012° |
γ | 90° |
Cell volume | 5322.4 ± 0.3 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0284 |
Residual factor for significantly intense reflections | 0.0246 |
Weighted residual factors for significantly intense reflections | 0.0497 |
Weighted residual factors for all reflections included in the refinement | 0.0508 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.176 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4087207.html
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