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Information card for entry 4087214
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Coordinates | 4087214.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | AS-51 |
---|---|
Formula | C24 H18 N O5 P W |
Calculated formula | C24 H18 N O5 P W |
SMILES | [W]([PH](N)C(c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])(C#[O])(C#[O])(C#[O])C#[O] |
Title of publication | 1,1′-Bifunctional Aminophosphane Complexes via N‒H Bond Insertions of a Li/Cl Phosphinidenoid Complex and First Studies on N/P Mono Functionalizations |
Authors of publication | Streubel, Rainer; Schmer, Alexander; Kyri, Andreas W.; Schnakenburg, Gregor |
Journal of publication | Organometallics |
Year of publication | 2017 |
a | 7.2639 ± 0.0009 Å |
b | 16.75 ± 0.002 Å |
c | 18.608 ± 0.002 Å |
α | 90° |
β | 98.941 ± 0.004° |
γ | 90° |
Cell volume | 2236.5 ± 0.5 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0306 |
Residual factor for significantly intense reflections | 0.025 |
Weighted residual factors for significantly intense reflections | 0.0614 |
Weighted residual factors for all reflections included in the refinement | 0.0637 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4087214.html
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