Information card for entry 4087217

Structure parameters

• Formula: C28 H26 N O5 P W
• Calculated formula: C28 H26 N O5 P W
• SMILES: C(C)N(CC)[PH](C(c1ccccc1)(c1ccccc1)c1ccccc1)[W](C#[O])(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: 1,1′-Bifunctional Aminophosphane Complexes via N‒H Bond Insertions of a Li/Cl Phosphinidenoid Complex and First Studies on N/P Mono Functionalizations
• Authors of publication: Streubel, Rainer; Schmer, Alexander; Kyri, Andreas W.; Schnakenburg, Gregor
• Journal of publication: Organometallics
• Year of publication: 2017
• a: 10.7367 ± 0.0007 Å
• b: 15.677 ± 0.001 Å
• c: 17.4538 ± 0.001 Å
• α: 104.204 ± 0.003°
• β: 98.484 ± 0.003°
• γ: 104.184 ± 0.003°
• Cell volume: 2692.9 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0605
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.1049
• Weighted residual factors for all reflections included in the refinement: 0.1134
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No