Information card for entry 4087477

Structure parameters

• Formula: C35 H57 N O4 W
• Calculated formula: C35 H57 N O4 W
• Title of publication: New Alkylidyne Complexes Featuring a Flexible Trianionic ONO3‒ Pincer-Type Ligand: Inorganic Enamine Effect versus Sterics in Electrophilic Additions
• Authors of publication: VenkatRamani, Sudarsan; Huff, Nicholas B.; Jan, Muhammad Tariq; Ghiviriga, Ion; Abboud, Khalil A.; Veige, Adam S.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 12
• Pages of publication: 2841
• a: 10.8745 ± 0.0012 Å
• b: 12.9169 ± 0.0015 Å
• c: 13.8354 ± 0.0016 Å
• α: 78.853 ± 0.002°
• β: 73.705 ± 0.002°
• γ: 73.025 ± 0.002°
• Cell volume: 1770.9 ± 0.4 ų
• Cell temperature: 233 ± 2 K
• Ambient diffraction temperature: 233 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0199
• Residual factor for significantly intense reflections: 0.0178
• Weighted residual factors for significantly intense reflections: 0.0461
• Weighted residual factors for all reflections included in the refinement: 0.0467
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No